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Article: Evaluation of resin adhesion to zirconia ceramic using some organosilanes

TitleEvaluation of resin adhesion to zirconia ceramic using some organosilanes
Authors
KeywordsBis-GMA
Luting cement
Silane
Silanization
Silica-coating
Zirconia
Issue Date2006
PublisherElsevier Inc. The Journal's web site is located at http://www.elsevier.com/locate/dental
Citation
Dental Materials, 2006, v. 22 n. 9, p. 824-831 How to Cite?
AbstractObjectives: This study evaluated and compared the effect of three trialkoxysilane coupling agents on the bond strength of a Bis-GMA-based unfilled resin and a dimethacrylate-based resin composite luting cement to a zirconia ceramics (Procera® AllZircon, Nobel Biocare, Göteborg, Sweden). Methods: Six square-shaped zirconia specimens were used for each test group, a total of 72 specimens. The specimens in each group were all assigned to air-borne alumina particle abrasion followed by tribochemical silica-coating and silanization with 1 vol% solutions of 3-methacryloyloxypropyltrimethoxysilane, 3-acryloyloxypropyltrimethoxysilane, or 3-isocyanatopropyltriethoxysilane in an ethanol-water mixture. The sample stubs were made of a Bis-GMA/MMA/DMAEMA resin or a commercial resin composite luting cement (RelyX™ ARC, 3M ESPE, Seefeld, Germany). They were bonded to the conditioned and silanized silica-coated zirconia specimens using polyethylene molds. All specimens were tested at dry and thermo-cycled (6000, 5-55 °C, 30 s) conditions. The shear bond strength of resin stubs to zirconia was measured in a universal testing machine (cross-head speed 1 mm/min). Results: In dry conditions, the highest shear bond strength was 9.7 MPa (S.D. 3.3 MPa), and for thermo-cycled samples 7.4 MPa (S.D. 2.4 MPa) was obtained with RelyX™ ARC cement with 3-methacryloyloxypropyltrimethoxysilane. In general, thermo-cycling decreased the bond strengths significantly for the Bis-GMA resin (ANOVA, p < 0.005). The resin, cement and silanes differed significantly silanes (ANOVA, p < 0.005). All samples silanized with 3-isocyanatopropyltriethoxysilane de-bonded during thermo-cycling. De-bonding was dominantly due to adhesive failure. Significance: Bonding of the experimental resin and commercial cement to silica-coated zirconia is effective with 3-methacryloyloxypropyltrimethoxysilane or 3-methacryloyloxypropyltrimethoxysilane, but not with 3-isocyanatopropyltriethoxysilane. © 2005 Academy of Dental Materials.
Persistent Identifierhttp://hdl.handle.net/10722/154417
ISSN
2023 Impact Factor: 4.6
2023 SCImago Journal Rankings: 1.186
ISI Accession Number ID
References

 

DC FieldValueLanguage
dc.contributor.authorMatinlinna, JPen_US
dc.contributor.authorHeikkinen, Ten_US
dc.contributor.authorÖzcan, Men_US
dc.contributor.authorLassila, LVJen_US
dc.contributor.authorVallittu, PKen_US
dc.date.accessioned2012-08-08T08:25:12Z-
dc.date.available2012-08-08T08:25:12Z-
dc.date.issued2006en_US
dc.identifier.citationDental Materials, 2006, v. 22 n. 9, p. 824-831en_US
dc.identifier.issn0109-5641en_US
dc.identifier.urihttp://hdl.handle.net/10722/154417-
dc.description.abstractObjectives: This study evaluated and compared the effect of three trialkoxysilane coupling agents on the bond strength of a Bis-GMA-based unfilled resin and a dimethacrylate-based resin composite luting cement to a zirconia ceramics (Procera® AllZircon, Nobel Biocare, Göteborg, Sweden). Methods: Six square-shaped zirconia specimens were used for each test group, a total of 72 specimens. The specimens in each group were all assigned to air-borne alumina particle abrasion followed by tribochemical silica-coating and silanization with 1 vol% solutions of 3-methacryloyloxypropyltrimethoxysilane, 3-acryloyloxypropyltrimethoxysilane, or 3-isocyanatopropyltriethoxysilane in an ethanol-water mixture. The sample stubs were made of a Bis-GMA/MMA/DMAEMA resin or a commercial resin composite luting cement (RelyX™ ARC, 3M ESPE, Seefeld, Germany). They were bonded to the conditioned and silanized silica-coated zirconia specimens using polyethylene molds. All specimens were tested at dry and thermo-cycled (6000, 5-55 °C, 30 s) conditions. The shear bond strength of resin stubs to zirconia was measured in a universal testing machine (cross-head speed 1 mm/min). Results: In dry conditions, the highest shear bond strength was 9.7 MPa (S.D. 3.3 MPa), and for thermo-cycled samples 7.4 MPa (S.D. 2.4 MPa) was obtained with RelyX™ ARC cement with 3-methacryloyloxypropyltrimethoxysilane. In general, thermo-cycling decreased the bond strengths significantly for the Bis-GMA resin (ANOVA, p < 0.005). The resin, cement and silanes differed significantly silanes (ANOVA, p < 0.005). All samples silanized with 3-isocyanatopropyltriethoxysilane de-bonded during thermo-cycling. De-bonding was dominantly due to adhesive failure. Significance: Bonding of the experimental resin and commercial cement to silica-coated zirconia is effective with 3-methacryloyloxypropyltrimethoxysilane or 3-methacryloyloxypropyltrimethoxysilane, but not with 3-isocyanatopropyltriethoxysilane. © 2005 Academy of Dental Materials.en_US
dc.languageengen_US
dc.publisherElsevier Inc. The Journal's web site is located at http://www.elsevier.com/locate/dentalen_US
dc.relation.ispartofDental Materialsen_US
dc.subjectBis-GMA-
dc.subjectLuting cement-
dc.subjectSilane-
dc.subjectSilanization-
dc.subjectSilica-coating-
dc.subjectZirconia-
dc.subject.meshAdhesivenessen_US
dc.subject.meshBisphenol A-Glycidyl Methacrylateen_US
dc.subject.meshDental Bondingen_US
dc.subject.meshDental Porcelainen_US
dc.subject.meshDental Stress Analysisen_US
dc.subject.meshMethacrylates - Chemistryen_US
dc.subject.meshMicroscopy, Electron, Scanningen_US
dc.subject.meshOrganophosphorus Compounds - Chemistryen_US
dc.subject.meshPilot Projectsen_US
dc.subject.meshPolyethylene Glycolsen_US
dc.subject.meshPolymethacrylic Acidsen_US
dc.subject.meshResin Cementsen_US
dc.subject.meshShear Strengthen_US
dc.subject.meshSilanes - Chemistryen_US
dc.subject.meshSurface Tensionen_US
dc.subject.meshZirconiumen_US
dc.titleEvaluation of resin adhesion to zirconia ceramic using some organosilanesen_US
dc.typeArticleen_US
dc.identifier.emailMatinlinna, JP:jpmat@hku.hken_US
dc.identifier.authorityMatinlinna, JP=rp00052en_US
dc.description.naturelink_to_subscribed_fulltexten_US
dc.identifier.doi10.1016/j.dental.2005.11.035en_US
dc.identifier.pmid16388846-
dc.identifier.scopuseid_2-s2.0-33746653356en_US
dc.relation.referenceshttp://www.scopus.com/mlt/select.url?eid=2-s2.0-33746653356&selection=ref&src=s&origin=recordpageen_US
dc.identifier.volume22en_US
dc.identifier.issue9en_US
dc.identifier.spage824en_US
dc.identifier.epage831en_US
dc.identifier.isiWOS:000240530100005-
dc.publisher.placeUnited Statesen_US
dc.identifier.scopusauthoridMatinlinna, JP=6602419428en_US
dc.identifier.scopusauthoridHeikkinen, T=14053957600en_US
dc.identifier.scopusauthoridÖzcan, M=7102067681en_US
dc.identifier.scopusauthoridLassila, LVJ=6603761779en_US
dc.identifier.scopusauthoridVallittu, PK=7006138548en_US
dc.identifier.issnl0109-5641-

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