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Article: Synthesis and X-ray structures of rhenium(I) carbonyl aminoalkoxide and aminocarboxylate complexes

TitleSynthesis and X-ray structures of rhenium(I) carbonyl aminoalkoxide and aminocarboxylate complexes
Authors
KeywordsOxidative alkoxylation
Amine-oxide
Aminoalkoxide
Aminocarboxylate
Rhenium
Carbonyl
Issue Date2006
Citation
Inorganica Chimica Acta, 2006, v. 359, n. 11, p. 3754-3762 How to Cite?
AbstractThe complexes [Re{MeN(CH2CH2O)(CH2CH2OH)-κ3N,O,O}(CO)3] (1), [Re{N(CH2CH2O)(CH2CH2OH)2-κ3N,O,O}(CO)3] (2), [Me3NH]2[(OC)3Re{N(CH2CO2)2-κ3N,O,O}CH2CH2{N(CH2CO2)2-κ3N,O,O}Re(CO)3] (3), [Me3NH]2[Re2{μ2-2,6-(O2C)2(C5H3N)-κ3N,O,O}2(CO)6] (4) and [Re2{μ2-2,6-(OCH2)(C5H3N)(CH2OH)-κ2N,O}2(CO)6] (5) were synthesized in high yields via the reactions of [Re2(CO)10] and Me3NO with MeN(CH2CH2OH)2, N(CH2CH2OH)3, EDTA, pyridine-2,6-dicarboxylic acid and pyridine-2,6-dimethanol, respectively. Complexes 1-5 were characterized by IR and 1H NMR spectroscopy, elemental analysis and X-ray crystallography. © 2006 Elsevier B.V. All rights reserved.
Persistent Identifierhttp://hdl.handle.net/10722/237571
ISSN
2020 Impact Factor: 2.545
2015 SCImago Journal Rankings: 0.584
ISI Accession Number ID

 

DC FieldValueLanguage
dc.contributor.authorWang, Wenwu-
dc.contributor.authorAndy Hor, T. S.-
dc.contributor.authorYan, Yaw Kai-
dc.date.accessioned2017-01-16T06:09:52Z-
dc.date.available2017-01-16T06:09:52Z-
dc.date.issued2006-
dc.identifier.citationInorganica Chimica Acta, 2006, v. 359, n. 11, p. 3754-3762-
dc.identifier.issn0020-1693-
dc.identifier.urihttp://hdl.handle.net/10722/237571-
dc.description.abstractThe complexes [Re{MeN(CH2CH2O)(CH2CH2OH)-κ3N,O,O}(CO)3] (1), [Re{N(CH2CH2O)(CH2CH2OH)2-κ3N,O,O}(CO)3] (2), [Me3NH]2[(OC)3Re{N(CH2CO2)2-κ3N,O,O}CH2CH2{N(CH2CO2)2-κ3N,O,O}Re(CO)3] (3), [Me3NH]2[Re2{μ2-2,6-(O2C)2(C5H3N)-κ3N,O,O}2(CO)6] (4) and [Re2{μ2-2,6-(OCH2)(C5H3N)(CH2OH)-κ2N,O}2(CO)6] (5) were synthesized in high yields via the reactions of [Re2(CO)10] and Me3NO with MeN(CH2CH2OH)2, N(CH2CH2OH)3, EDTA, pyridine-2,6-dicarboxylic acid and pyridine-2,6-dimethanol, respectively. Complexes 1-5 were characterized by IR and 1H NMR spectroscopy, elemental analysis and X-ray crystallography. © 2006 Elsevier B.V. All rights reserved.-
dc.languageeng-
dc.relation.ispartofInorganica Chimica Acta-
dc.subjectOxidative alkoxylation-
dc.subjectAmine-oxide-
dc.subjectAminoalkoxide-
dc.subjectAminocarboxylate-
dc.subjectRhenium-
dc.subjectCarbonyl-
dc.titleSynthesis and X-ray structures of rhenium(I) carbonyl aminoalkoxide and aminocarboxylate complexes-
dc.typeArticle-
dc.description.naturelink_to_subscribed_fulltext-
dc.identifier.doi10.1016/j.ica.2006.03.027-
dc.identifier.scopuseid_2-s2.0-33745712219-
dc.identifier.volume359-
dc.identifier.issue11-
dc.identifier.spage3754-
dc.identifier.epage3762-
dc.identifier.isiWOS:000239475800040-
dc.identifier.issnl0020-1693-

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