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Article: Synthesis and mass spectrometry of 2-hydroxyethyl 1-aminoalkylphosphonates
| Title | Synthesis and mass spectrometry of 2-hydroxyethyl 1-aminoalkylphosphonates |
|---|---|
| Authors | |
| Keywords | Synthesis Mannich-type reaction Multiple component condensation Aminoalkylphosphonic acid Amino acid Mass spectrometry Alkylphosphonate |
| Issue Date | 2007 |
| Citation | Phosphorus, Sulfur and Silicon and the Related Elements, 2007, v. 182, n. 1, p. 25-33 How to Cite? |
| Abstract | Mannich-type condensation of benzyl carbamate, aldehydes, and chlorophosphite has been widely used in the synthesis of 1-(N- benzyloxycarbonylamino)arylmethyl-phosphonic derivatives. Reactions of benzyl carbamate, aldehydes, and cyclic chlorophosphite 2-chloro-1,3,2-dioxaphospholane were conducted in benzene to afford a mixture of benzyl [(2-oxido-1,3,2- dioxaphospholane-2-yl)arylmethyl]-carbamates and 2-hydroxyethyl 1-(N-benzoxycarbonylamino)arylmethylphos-phonate monoesters. 2-hydroxyethyl 1-(N-benzoxycarbonylamino)arylmethylphos-phonate monoesters were obtained exclusively after the addition of water under stirring. The reaction mechanism was discussed. Their mass spectrometric fragmentations were also described. |
| Persistent Identifier | http://hdl.handle.net/10722/291769 |
| ISSN | 2023 Impact Factor: 1.4 2023 SCImago Journal Rankings: 0.240 |
| ISI Accession Number ID |
| DC Field | Value | Language |
|---|---|---|
| dc.contributor.author | Cai, Shuzong | - |
| dc.contributor.author | Yin, Wei | - |
| dc.contributor.author | Ma, Yuan | - |
| dc.contributor.author | Liu, Han | - |
| dc.contributor.author | Zhao, Yufen | - |
| dc.contributor.author | Xu, Jiaxi | - |
| dc.date.accessioned | 2020-11-17T14:55:04Z | - |
| dc.date.available | 2020-11-17T14:55:04Z | - |
| dc.date.issued | 2007 | - |
| dc.identifier.citation | Phosphorus, Sulfur and Silicon and the Related Elements, 2007, v. 182, n. 1, p. 25-33 | - |
| dc.identifier.issn | 1042-6507 | - |
| dc.identifier.uri | http://hdl.handle.net/10722/291769 | - |
| dc.description.abstract | Mannich-type condensation of benzyl carbamate, aldehydes, and chlorophosphite has been widely used in the synthesis of 1-(N- benzyloxycarbonylamino)arylmethyl-phosphonic derivatives. Reactions of benzyl carbamate, aldehydes, and cyclic chlorophosphite 2-chloro-1,3,2-dioxaphospholane were conducted in benzene to afford a mixture of benzyl [(2-oxido-1,3,2- dioxaphospholane-2-yl)arylmethyl]-carbamates and 2-hydroxyethyl 1-(N-benzoxycarbonylamino)arylmethylphos-phonate monoesters. 2-hydroxyethyl 1-(N-benzoxycarbonylamino)arylmethylphos-phonate monoesters were obtained exclusively after the addition of water under stirring. The reaction mechanism was discussed. Their mass spectrometric fragmentations were also described. | - |
| dc.language | eng | - |
| dc.relation.ispartof | Phosphorus, Sulfur and Silicon and the Related Elements | - |
| dc.subject | Synthesis | - |
| dc.subject | Mannich-type reaction | - |
| dc.subject | Multiple component condensation | - |
| dc.subject | Aminoalkylphosphonic acid | - |
| dc.subject | Amino acid | - |
| dc.subject | Mass spectrometry | - |
| dc.subject | Alkylphosphonate | - |
| dc.title | Synthesis and mass spectrometry of 2-hydroxyethyl 1-aminoalkylphosphonates | - |
| dc.type | Article | - |
| dc.description.nature | link_to_subscribed_fulltext | - |
| dc.identifier.doi | 10.1080/10426500600865251 | - |
| dc.identifier.scopus | eid_2-s2.0-33845289798 | - |
| dc.identifier.volume | 182 | - |
| dc.identifier.issue | 1 | - |
| dc.identifier.spage | 25 | - |
| dc.identifier.epage | 33 | - |
| dc.identifier.eissn | 1563-5325 | - |
| dc.identifier.isi | WOS:000242549600004 | - |
| dc.identifier.issnl | 1026-7719 | - |