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Article: Isochronous and Anisochronous O-Methylene Protons in Cyclic and Acyclic Acetals
Title | Isochronous and Anisochronous O-Methylene Protons in Cyclic and Acyclic Acetals |
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Authors | |
Issue Date | 1969 |
Citation | Journal of the American Chemical Society, 1969, v. 91, n. 17, p. 4722-4724 How to Cite? |
Abstract | Configurational assignments are made to some cyclic and acyclic acetals on the basis of the nature of the signals for their O-methylene protons in their pmr spectra. The three known 4,5: 9,10-biscyclohexano-1,3,6,8-tetraoxacyclodecanes are assigned the trans-syn-trans, trans-anti-trans, and cis-anti-cis configurations and the di-(trans-2-hydroxycyclohexyloxy)methanes with mp 80-82° and mp 102.5-103.5° are assigned to the meso form and dl modification, respectively. © 1969, American Chemical Society. All rights reserved. |
Persistent Identifier | http://hdl.handle.net/10722/332723 |
ISSN | 2023 Impact Factor: 14.4 2023 SCImago Journal Rankings: 5.489 |
DC Field | Value | Language |
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dc.contributor.author | Grindley, T. B. | - |
dc.contributor.author | Stoddart, J. F. | - |
dc.contributor.author | Szarek, W. A. | - |
dc.date.accessioned | 2023-10-06T05:13:46Z | - |
dc.date.available | 2023-10-06T05:13:46Z | - |
dc.date.issued | 1969 | - |
dc.identifier.citation | Journal of the American Chemical Society, 1969, v. 91, n. 17, p. 4722-4724 | - |
dc.identifier.issn | 0002-7863 | - |
dc.identifier.uri | http://hdl.handle.net/10722/332723 | - |
dc.description.abstract | Configurational assignments are made to some cyclic and acyclic acetals on the basis of the nature of the signals for their O-methylene protons in their pmr spectra. The three known 4,5: 9,10-biscyclohexano-1,3,6,8-tetraoxacyclodecanes are assigned the trans-syn-trans, trans-anti-trans, and cis-anti-cis configurations and the di-(trans-2-hydroxycyclohexyloxy)methanes with mp 80-82° and mp 102.5-103.5° are assigned to the meso form and dl modification, respectively. © 1969, American Chemical Society. All rights reserved. | - |
dc.language | eng | - |
dc.relation.ispartof | Journal of the American Chemical Society | - |
dc.title | Isochronous and Anisochronous O-Methylene Protons in Cyclic and Acyclic Acetals | - |
dc.type | Article | - |
dc.description.nature | link_to_subscribed_fulltext | - |
dc.identifier.doi | 10.1021/ja01045a024 | - |
dc.identifier.scopus | eid_2-s2.0-33947301078 | - |
dc.identifier.volume | 91 | - |
dc.identifier.issue | 17 | - |
dc.identifier.spage | 4722 | - |
dc.identifier.epage | 4724 | - |
dc.identifier.eissn | 1520-5126 | - |