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Article: Conformational behaviour of medium-sized rings. Part 14. tetra- anthranilides

TitleConformational behaviour of medium-sized rings. Part 14. tetra- anthranilides
Authors
Hoorfar, AlirezaOllis, W. DavidStoddart, J. Fraser
Issue Date1982
Citation
Journal of the Chemical Society, Perkin Transactions 1, 1982, p. 1721-1726 How to Cite?
DOI: http://dx.doi.org/10.1039/P19820001721
AbstractThe stepwise synthesis of N, N′, N″-trimethyltetra-anthranilide (13) is reported and the temperature dependence of the1H n.m.r. spectrum of N-benzyl-N, N′, N″, N‴-trimethyltetra-anthranilide (15) is interpreted in terms of equilibration between three diastereoisomeric conformations in solution. Although there is1H n.m.r. spectral evidence for the presence in solution at room temperature of at least six conformational diastereoisomers of (13), N, N″, N‴- tetramethyltetra-anthranilide (14) appears to adopt a single conformation of high symmetry in solution. © Royal Society of Chemistry.
Persistent Identifierhttp://hdl.handle.net/10722/332804
ISSN
1470-4358
ISI Accession Number ID
WOS:A1982PC03300006

 

DC FieldValueLanguage
dc.contributor.authorHoorfar, Alireza-
dc.contributor.authorOllis, W. David-
dc.contributor.authorStoddart, J. Fraser-
dc.date.accessioned2023-10-06T05:14:24Z-
dc.date.available2023-10-06T05:14:24Z-
dc.date.issued1982-
dc.identifier.citationJournal of the Chemical Society, Perkin Transactions 1, 1982, p. 1721-1726-
dc.identifier.issn1470-4358-
dc.identifier.urihttp://hdl.handle.net/10722/332804-
dc.description.abstractThe stepwise synthesis of N, N′, N″-trimethyltetra-anthranilide (13) is reported and the temperature dependence of the<sup>1</sup>H n.m.r. spectrum of N-benzyl-N, N′, N″, N‴-trimethyltetra-anthranilide (15) is interpreted in terms of equilibration between three diastereoisomeric conformations in solution. Although there is<sup>1</sup>H n.m.r. spectral evidence for the presence in solution at room temperature of at least six conformational diastereoisomers of (13), N, N″, N‴- tetramethyltetra-anthranilide (14) appears to adopt a single conformation of high symmetry in solution. © Royal Society of Chemistry.-
dc.languageeng-
dc.relation.ispartofJournal of the Chemical Society, Perkin Transactions 1-
dc.titleConformational behaviour of medium-sized rings. Part 14. tetra- anthranilides-
dc.typeArticle-
dc.description.naturelink_to_subscribed_fulltext-
dc.identifier.doi10.1039/P19820001721-
dc.identifier.scopuseid_2-s2.0-37049108723-
dc.identifier.spage1721-
dc.identifier.epage1726-
dc.identifier.isiWOS:A1982PC03300006-

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